Superior lab efficiency in the determination of organic pollutants from environmental matrices

Determination of organic pollutants in environmental matrices is a common task for thousands of laboratories worldwide, as it leads to controlling and protecting our environment from high levels of contaminants. This analysis is often done to evaluate the effectiveness of a remediation process, to assess the contamination in waste, in waste landfills and for general environmental monitoring. Therefore, every day environmental laboratories deal with several challenges to ensure high quality data and fast turnaround time while maintaining their competitiveness.
Extraction of pollutants from solid matrices is often performed with techniques that limit the productivity and have high running costs.
Milestone listened to the needs of environmental laboratory professionals by developing the ETHOS X with the fastEX-24eT rotor, which allows for simultaneous extraction of 24 samples in 40 minutes with minimal solvent usage. By using large volume disposable glass vials, the fastEX-24eT rotor simplifies handling and allows to achieve lower detection limits.
Typical applications of microwave-assisted solvent extraction include chlorinated pesticides, semi-volatile organics, PAHs, PCBs, chlorinated herbicides, phenols, organophosphorus pesticides, dioxins and furans.
  • High productivity. 24 samples in 40 minutes.
  • Low running cost. Substantial reduction in solvent.
  • Ease of use. Disposable glass vials.
  • Larger sample amount. Up to 30 grams.
  • Compliance. Fully compliant with US EPA 3546 Method.
  • Reliability. Consistent and reproducible results.
High throughput.
24 samples in 40 minutes.
Superior return of investment.
Substantial reduction in solvent.
Simple handling.
Disposable glass vials.
Consintency & Reproducibility.
Consistent and reproducible results.
Safety & Reliability.

Book

Microwave Green Extraction

Microwave Green Extraction

Modernizing Analysis of Trace Organic Compounds in Environmental Matrices.

Webinar

Learn how to improve the extraction process

The true importance of sample prep processing procedures and its impact on the analysis quality.

Achieving lower detection limits
with higher sample amount.

The ETHOS X with fastEX-24eT rotor extracts up to 30 grams of sample with minimal solvent volume, helping analysts to accomplish their tasks.
The Milestone fastEX-24eT rotor uses disposable glass vials, eliminating the need for cleaning and the possibility of memory effect between different runs. The 100 mL vials can accommodate the extraction of a large sample amount. The easy to handle and affordable cost of the vials leads to high productivity at a very low running cost.
fastEX-24eT rotor

Large sample amount
in disposable glass vials.

The ETHOS X with fastEX-24 rotor extracts up to 30 grams of sample with minimal solvent volume, helping analysts to accomplish their tasks.
The Milestone fastEX-24 rotor uses disposable glass vials, eliminating the need for cleaning and the possibility of memory effect between different runs. The 100 mL vials can accommodate the extraction of a large sample amount. The easy to handle and affordable cost of the vials leads to high productivity at a very low running cost.
24 SAMPLES IN < 1 HOUR
fastEX-24 rotor

Ease of use with disposable glass vials

The ETHOS X operation is simple: samples are loaded into large volume disposable glass vials with appropriate solvent mixture, placed into the Weflon vessel and sealed. The unique vessel design, in combination with the accurate temperature control, enables extraction of different matrices simultaneously, which enhances the lab's workflow. The accurate contactless temperature sensor ensures full control of the extraction cycle in all positions and displays real-time the temperature of all samples on the dedicated user interface. The 100-mL glass disposable vials accommodate large sample amounts of up to 30 g, enabling lower detection limits with minimal solvent volume. In addition, the memory effects often observed with other technologies are eliminated, expediting even trace analysis of challenging species such as dioxins.

Productivity

Although new extraction technologies have been developed in recent years, they have fallen short on addressing the needs of environmental labs. The ETHOS X with fastEX-24eT overcomes productivity limitations of other conventional approaches by enabling the extraction of a large number of samples in a single workday. Other technologies process one sample at a time sequentially, requiring long extraction cycles. The ETHOS X simultaneously processes 24 samples in only 40 minutes and eliminates cleaning steps by using disposable glass vials. The graphic below compares the typical daily productivity using the Milestone ETHOS X, Sequential Pressurized Liquid Extraction and Soxhlet.
Productivity
Productivity based on 8 hours working shift. 24 samples requiring 40 minutes with the ETHOS X, 240 minutes with Sequential Pressurized Liquid Extraction and multiple hours with Soxhlet.

Consistency

Data quality and reliability are key features for environmental labs. The ETHOS X with the fastEX-24eT rotor provides fast, accurate and precise analysis. The vessels, in combination with the temperature sensor, allow to simultaneously process various matrices ensuring optimal extraction efficiency. In addition, the unique design of the fastEX-24eT rotor with its large volume disposable glass vials (100 mL) eliminates cross contamination and memory effect, providing reproducible results.
Consistency and Reliability
Milestone ETHOS X recovery study and comparison vs Soxhlet for various organic compounds.

Compliance

Several official methods describe the use of microwave closed-vessel technology to enhance the extraction efficiency of organic pollutants, such as US EPA 3546, ASTM and other national methods. The Table 1 reports the typical extraction conditions. The ETHOS X with fastEX-24eT further enhances the performance of microwave technology for the extraction of water-insoluble or slightly water-soluble organic compounds from soils, clays, sediments, sludges, and solid wastes. In fact, the ETHOS X with fastEX-24eT can be used for solvent extraction of chlorinated pesticides, semi-volatile organics, PAHs, PCBs, chlorinated herbicides, phenols, organophosphorus pesticides, dioxins and furans.

Greater return on investment

The competitive nature of the environmental analysis market requires today's laboratories to have innovative solutions that provide faster turnaround times. With throughput capabilities of 24 samples in only 40 minutes, the ETHOS X with fastEX-24eT reduces overall analysis costs by increasing productivity. The combination of lower solvent volumes, less maintenance needs, and the use of inexpensive disposable glass vials decreases the cost per sample to enhance your lab's competitiveness and profitability.
Greater return on investment

Real-life experiences and successes

  • IREN laboratories process waste samples with high plastic content

    IREN laboratories process waste samples with high plastic content
    The laboratories of the Iren Ambiente are able to offer environmental analysis and consultancy services concerning water, soil, waste and compost. The main reason why they decided to adopt the m...
  • SYNLAB lab profile

    SYNLAB lab profile
    SYNLAB Sweden is focused on the determination of organic pollutants in different matrices, such as Dioxins and Furans, PAH’s and PCB’s. The Milestone ETHOS X microwave system with the fastEX-24 rot...
  • ACEA lab profile

    ACEA lab profile
    The ACEA Group deals with waste management, handling over 1 million tons of waste every year. Its activities are mainly concentrated in Italy but they are also present in some Latin American co...
  • EnviroTest lab profile

    EnviroTest lab profile
    EnviroTest accomplished their mission by adding a full Organic Department, gaining a reputation as a trusted leader in water and soil testing services for the Hudson Valley serving NY, NJ and CT. ...
  • Ecosistem lab profile

    Ecosistem lab profile
    Ecosistem S.r.l. is a consulting company specializing in chemical and microbiological analysis both in terms of environment and workplace safety. The company’s mission is to be a point of reference...

SFS-24

SIMULTANEOUS FILTRATION SYSTEM

The analysis of organic pollutants in environmental matrices, such as soils and sediments, includes the filtration step, after a solvent extraction process. The Milestone Simultaneous Filtration System (SFS) is a compact and complete workstation to filter up to 24 samples simultaneously in a few minutes. Samples are filtered into standard evaporation tubes, using the Milestone disposable funnels, providing easier handling and reducing fume hood space.
SFS-24 Simultaneous Filtration System
  • SIMULTANEOUS FILTRATION
  • UP TO 24 SAMPLES IN FEW MINUTES
  • COMPACT & ERGONOMIC DESIGN
  • BETTER WORKFLOW
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