Microwave extraction technology enables to process difficult organic matrices eliminating tedious vessel cleaning steps
CUSTOMER
The ACEA Group deals with waste management, handling
over 1 million tons of waste every year. Since 2006, it has
been managing waste-to-energy plants, composting plants
and in 2019 the company also entered the plastic treatment
sector. ACEA operates two incinerators that burn waste and
pulp.
ACEA is also the top national operator in the water sector,
serving 9 million customers in the Lazio, Tuscany, Umbria,
Molise and Campania regions of Italy.
The laboratory gets involved in several aspects: water
analysis; characterization of wastes from purification plants
(exhausted sewage sludge, soils) and from incinerators
(ashes, soils, slags). Moreover, it is active in the industrial
emissions and environmental monitoring.
CHALLENGE
The ACEA lab performs SVOCs analysis on solid waste and
it is equipped for organic pollutant testing with the latest
instrumentation. The previous adopted technique for the extraction process
was Pressurized Liquid Extraction technique (PLE).
The main reason why they decided
to switch to microwave assisted
extraction technique was the need
to reduce time per analysis and
to process some of the most
difficult and polluted matrices
avoiding high maintenance costs
and tedious cleaning steps.
From the customer voice:
“The extraction time per sample was reduced by
90% with the ETHOS X, thanks to the simplified
handling and the elimination of the cleaning steps”
IMPLEMENTATION of ETHOS X with fastEX-24 rotor
The main benefits achieved by ACEA are the following:
Reduced extraction time. PLE is able to process 24 samples in 6 hours, while ETHOS X is able to process 24 samples in less than 1 hour.
Wide application range. Thanks to the robustness of the ETHOS X hardware, ACEA could process all kind of solid matrices, even those with high plastic content or highly polluted ones, eliminating any clogging problem that typically occurs with the previous sequential technique.
No cleaning of vials. A common and very critical issue for all sample preparation techniques is the subsequent memory effect/carry-over in the extraction cells. For instance, the stability of dioxins requires long and tedious cleaning procedures of the extraction vessels. The implementation of the fastEX-24 rotor eliminates the cleaning steps by using disposable and inexpensive glass vials as reaction vessels.
ETHOS X offers superior lab efficiency in the determination of organic pollutants with microwave green extraction technique. Typical applications include chlorinated pesticides, semi-volatile organics, PAHs, PCBs, chlorinated herbicides, phenols, organophosphorus pesticides, dioxins and furans