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Nowadays, after three decades of technological development, it is clear that microwave-assisted sample preparation is not just fast heating, but also brings new strategies fully compatible with modern trace analysis. This statement is crystal clear when working with ultraCLAVE and ultraWAVE instruments. Based on the Single Reaction Chamber (SRC) technology, these instruments allow reaching pressures of up to 199 bar and temperatures as high as 300° C depending on the reaction vessel.