USP 232 / 233 and ICH Q3D: Choose the right tools to implement these methods in your lab

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Priligy no script required express delivery WEBINAR: USP / and ICH Q3D: choose the right tools to implement these methods in your lab

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Elemental impurities in pharmaceutical products can be introduced from a number of sources, including catalysts, raw materials, production processes, and packaging materials. The implementation of the new USP chapters <232> and <233>, and ICH Q3D guidelines on elemental impurities, in January 2018, will redefine how the pharmaceutical industry tests for elemental impurities in drug products. The quantitative determination of elemental impurities has to be conducted using appropriate procedures suitable for their intended purposes via ICP-MS / ICP-OES and will place a major emphasis on robust sample preparation.

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Milestone invites you to attend this Webinar, when we will present the new method requirements, define key parameters, and discuss considerations laboratories should make as they get themselves ready to implement the new methods and to consider the risk assessment on their pharmaceuticals. Through incorporating case studies, we will discuss the importance of sample preparation and the key parameters that have to be considered in order to choose the correct analytical method.

Attendees will receive the "Complete Sample Preparation Guide", the primer for QA/QC practitioners and Lab Managers with our compliments.

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Trace Metal Determination in Environmental Samples

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Many laboratories concerned with the analysis of elements in environmental samples, such as ground waters, industrial wastes, soils, sludge and sediment for trace metal analysis, work to United States Environmental Protection Agency (US EPA) method 6010C guidelines. Fast sample throughput and low cost analysis is desirable for these labs but can be challenging to achieve.

Milestone invites you to attend this Webinar, in which we will introduce effective techniques for safe and rapid microwave digestion and for direct mercury determination. You will discover how Milestone instruments can bring benefits to your lab routine. We will show you how to prepare your environmental samples and how to obtain good data quality during analysis.

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Webinar recording

Why is a direct mercury analyser the most popular choice for Hg determination in environmental samples?

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As more emphasis is placed on the monitoring of mercury emissions, both private and public institutions are looking at characterizing soil, sediments and waste water samples. Con- taminated soil has to be excavated and remediated, or depending on the level of contamination, disposed of as hazardous waste.
Several methods are available for mercury analysis in environmental samples such as waste water and soil. Most of these methods however, require elaborate preparation procedures that are labor intensive and consequently expensive.
Direct mercury analysis, as described in operazioni binaru EPA Method 7473, is an alternative to these methods and has been used successfully to determine total mercury in environmental samples.
This technique requires no sample preparation and delivers results in as little as 6 minutes per sample, making it signicantly faster than traditional wet chemistry.
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Complimentary, live webinar: Microwave technology applied to inorganic synthesis

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Microwave technology applied to inorganic synthesis: what is going to change?

Changing the conventional methodologies of inorganic synthesis to more environmental-friendly and cost effective methods has opened up new avenues to achieve an enhanced and novel sustainable chemistry, thus contributing to the preservation of the natural environment.

vip2Inorganic synthesis is an important branch of the chemical synthesis with the aim of the production of new materials with new functions for new applications.

These routes, such as the microwave assisted hydrothermal synthesis provide the use of microwaves combined with the efficiency of the hydrothermal method. This facilitate the engineering of a wide variety of high-quality materials such as nano-sized rare earth doped ceria with fluorite structure for SOFC electrolyte applications, BiFeO3 perovskite with multiferroic properties and H2V3O8 with one-dimensional (1D) nanostructure for lithium battery technology.

During this webinar, we will go through the complete and up-to-date possibilities offered by the combination of two rapid and “green chemistry” synthesis techniques: hydrothermal synthesis and microwave synthesis. The goal is to minimize heat exposure and reaction times for chemical synthesis. Moreover, the particle sizes and shapes of the product can be fine tuned by the synthesis parameters.

Take part in our complimentary, live webinar!

You’ll interact with the experts who are breaking ground in this field of research: Emilio Miguélez Morán, professor at University of Madrid and Diego Carnaroglio, PhD, synthesis specialist at Milestone Srl.

You’ll learn about the newest tools and technologies while gathering valuable tips and troubleshooting strategies for the applications most relevant to your processes.

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PRESENTERS
 
Diego Carnaroglio, PhD
Synthesis and Extraction Application Specialist
at Milestone
 
In 2011 he received the Degree in Chemistry at the University of Turin and in 2014 he received the Ph.D. in Pharmaceutical and Biomolecular Sciences at the same university under the guidance of Prof. Giancarlo Cravotto with a thesis titled “Key enabling technologies for green, highly competitive chemical processes”. His research activity is documented by 20 scientific papers and 1 book chapter, 11 posters and 10 oral communications at international conferences. His collaboration with the University of Turin is still active, in order to developed new sustainable and green microwave processes.

 
Emilio Morán Miguélez, Prof.
Universidad Complutense
of Madrid
 
Full professor of Chemistry at the Universidad Complutense in Madrid and Head of Department of Inorganic Chemistry. Prof. Morán is an expert in the microwave assisted inorganic synthesis and solid state synthesis, “Fast and Soft Chemistry”. His efforts are in the synthesis of material for technological application such as superconductors, magnetic materials and solid electrolites.
He is the evaluation expert for ANECA, ACAP, ACSUG, AVAP, ANEP quality agencies and his research activity is documented by more than 200 scientific papers and several plenary contributions to international conferences.
 

Webinar invitation: Clean Chemistry Tools for Atomic Spectroscopy

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The goal of our webinar is offering a practical guideline for analysts and for everyone interested in the evolution of sample preparation strategies.
In this webinar we discuss how to control contaminations and modern strategies for microwave-assisted sample preparation.


Discussions comprehend digestions with diluted acid solutions, microwave-assisted evaporation, microwave vessels with inserts, vapor phase microwave digestion, and single reaction vessel. Modern procedures for sample preparation fully compatible with multielement determinations are presented and experimental data are shown. Instruments and accessories for implementing these strategies will be presented.

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Watch It Again: Metal Detection in Foodstuffs?

Microwave digestion of food samples

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Low-level analysis of food matrices has placed a demand on manufacturers, testing laboratories, and instrumentation vendors worldwide. Stricter regulations, better analytical instrumentation, and greatly improved sample preparation (preanalytical) techniques have focused efforts to simplify and standardize these analyses.
Often overlooked, the preanalytical step determines the quality of the resulting data and requires careful attention to a number of details, including sample size, digestion parameters, and the level of detection needed.
This webinar will provide the background on the technologies used for microwave digestion and their advantages towards these food related issues. The latest developments regarding available instrument configurations, detection limits, sample prep, and more will be discussed.

Watch our a free webinar that focuses on: Foodstuff processing, element concentration limits, preanalytical steps, importance of sample prep in Trace Metals Analysis for ICP MS/OES, application issues: sample size, acid digestion volume, sample fat and organic content, contamination, throughput, and post-digestion residual carbon content.

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New horizons in microwave chemical synthesis

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10 November, 2015

How can this benefit your research?
… Imagine being able to perform complex reactions with one single platform. Overcome the limitation of conventional microwave synthesis devices thanks to flexiWAVE, a single microwave platform that allows the chemists to perform classic glassware and high-pressure synthesis, as well as solid-phase reactions in a single unit.
… Imagine being able to better control reactions to get faster results and screen multiple reactions simultaneously. synthWAVE enables to vary the solvent or catalyst or even how many different reactions can be run in a single reaction vessel - simultaneously.

WATCH OUR WEBCAST HERE

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How Do You Know Food Safety?

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WEBINAR: How do you know Food Safety? The evolution of mercury determination technology for Food Samples

Over time, inorganic mercury consumed by fish and marine animals gets converted to organic methyl mercury, which is extremely toxic. Methyl mercury poses a significant health risk, making mercury analysis of fish tissue a primary focal point of both private and public institutions.
In this webinar, we'll explore how direct mercury analysis addresses the challenges posed with conventional mercury techniques such as ICP-MS and CVAA, when analyzing mercury in food matrices, especially fish and biological tissue. We’ll explore:
• The impacts of mercury in the environment and growing concerns as it relates to fish and other aquatic life
• Precise and rapid determination of total mercury in Food, especially in fish and marine animals
• A look at the flexibility of an extremely wide dynamic detection range to analyze different matrices with varying mercury levels
• Tips and Techniques for running fish samples on a direct mercury analyzer

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Watch our webinar!

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WEBINAR: Metal Detection in Enviromental Samples? Make it accurate, productive and fast

Pollution due to human activities makes an attempt on the health of many elements: air, water and soil.

It is fundamental to analyse the presence of heavy metals and many laboratories take care of this important monitoring of the ecosystems. Many laboratories specialized in analysing environmental materials are equipping their lab with instrumentation capable to prepare samples before analysis.

Often overlooked, the preanalytical step determines the quality of the resulting data. With this webinar you will discover how Milestone instruments can bring benefits to your lab routine. We will show you how to prepare your environmental samples and how to obtain good data quality during analysis.

WATCH IT NOW and we will answer to the following questions: Do you know which is the best acid combination for metal recoveries in soil samples? Which temperature (and pressure) is necessary to obtain a good digestion for organic materials? Which is the best microwave configuration for your environmental lab? Do you know how to increase the productivity of your lab?

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Webinar: Novel solutions for increasing productivity in contract labs

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WEBINAR: Novel solutions for increasing productivity in commercial contract labs?

Without question, the ultimate goal of your lab should be to find a flexible, easy-to-use sample preparation solution for preparing any element, in a variety of matrices, over a wide concentration range.
Standardizing multi-element sample preparation to include little to no method development, the capability of processing mixed sample batches and simultaneous detection techniques offers a cost effective solution to increase laboratory productivity.
Milestone provide complete solutions for today’s contract laboratory needs.
This interactive webinar will highlight how you can advance your contract lab’s capabilities with novel sample prep solutions.

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Webinar: Analysis of Mercury in your environmental samples?

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WEBINAR: Analysis of Mercury in your environmental samples?

Mercury from natural and anthropogenic sources such as soil, rocks, and coal fired plants ultimately gets washed into the water bodies around us and enters our food chain. Over time, inorganic mercury consumed by fish and marine animals gets converted to organic methyl mercury, which is extremely toxic.
Methyl mercury poses a significant health risk, making mercury analysis of fish tissue a primary focal point of both private and public institutions.

In this webinar, we'll explore how direct mercury analysis addresses the challenges posed with conventional mercury techniques such as ICP-MS and CVAA, when analyzing environmental samples.

Watch webinar recording now. Ask This email address is being protected from spambots. You need JavaScript enabled to view it. for the password.

 

 


Webinar: Be ready for USP 232 & 233!

Microwave digestion of pharma samples

WEBINAR: Practical Guidance on Sample Preparation of Elemental Impurities in Pharmaceutical Samples

Impurities in pharmaceutical products are of great concern not only due to the inherent toxicity of certain contaminats, but also due to the adverse effect that contaminats may have on drug stability and shelf-life.
The current USP “heavy metals limit test” is due to be replaced with new USP 232 General Chapters USP (Limits) and USP 233 (Procedures revision).
This webinar will provide the background on the development of the new General Chapters and explain how closed vessel microwave digestion can address the requirements of the proposed new methods. The latest developments regarding detection limits, implementation dates, and more will be discussed. In addition, this webinar will take an in depth look at a new approach that has revolutionized how labs operate removing all the barriers of traditional techniques while offering high ROI for labs needing high throughput and mixed batch runs.

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Metal Detection in Foodstuffs? Make it accurate, productive and fast.

Microwave digestion of food samples

WEBINAR: Metal Detection in Foodstuffs? Make it accurate, productive and fast.

Low-level analysis of food matrices has placed a demand on manufacturers, testing laboratories, and instrumentation vendors worldwide. Stricter regulations, better analytical instrumentation, and greatly improved sample preparation (preanalytical) techniques have focused efforts to simplify and standardize these analyses.
Often overlooked, the preanalytical step determines the quality of the resulting data and requires careful attention to a number of details, including sample size, digestion parameters, and the level of detection needed.
This webinar will provide the background on the technologies used for microwave digestion and their advantages towards these food related issues. The latest developments regarding available instrument configurations, detection limits, sample prep, and more will be discussed.

Join us for a free webinar that will focus on: Foodstaff processing, element concentration limits, preanalytical steps, importance of sample prep in Trace Metals Analysis for ICP MS/OES, application issues: sample size, acid digestion volume, sample fat and organic content, contamination, throughput, and post-digestion residual carbon content.

WATCH THE RECORDING NOW

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Sample preparation for USP 232 & 233

USP

The United States Pharmacopoeia (USP) is in the process of developing a new test for inorganic impurities in pharmaceutical products and their ingredients. The current USP “heavy metals limit test” is widely acknowledged to be inadequate in terms of scope, accuracy, sensitivity, and specificity, and is due to be replaced with new USP 232 General Chapters USP (Limits) and USP 233 (Procedures revision). The new methods will address the limitations of the current method, in particular with respect to the list of analytes, sample preparation, retention of volatile analytes, and the use of closed vessel sample digestion and modern instrumental techniques for the accurate recovery and determination of individual analyte concentrations.

A large part of samples will required closed vessel microwave digestion.

Milestone with the most complete digestion line and a unique experience in sample preparation provides a complete solution to match the new USP requirements. 

Milestone has designed a suitable configuration of the ETHOS UPUltraWAVE and ETHOS EASY to fully comply the specifications of the new USP chapters 232 and 233. 
The Milestone USP packages include:

  • - Dedicated application notes
  • - Free method development on your own samples
  • - IQ/OQ
  • - Installation and training done by a factory trained specialist
  • - Application support directly from the factory

US Pharmacopeia links:
Procedures: Revision Bulletin: Elemental Impurities Chapter 232 & 233

Be ready for the implementation of the USP chapters 232 & 233!
Meet our Product Specialist in your country to get additional information and to organize a demonstration.


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